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INTERNATIONAL JOURNAL OF PHARMACEUTICAL RESEARCH

A Step Towards Excellence
Published by : Advanced Scientific Research
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0975-2366
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IJPR 9[3] July - September 2017 Special Issue

July - September 9[3] 2017

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Synthesis , Characterization , Antimicrobial Studies of New5-[(2E)-2-{(2Z)-2-[2-(5-sulfanyl-1,3,4- thiadiazol-2- yl)hydrazinylidene]ethylidene}hydrazinyl]-1,3,4- thiadiazole-2-thioland their transition metal complexes

Author: RASHA. N.ALJABERY, AZHARHAMEEDGATEA, IBRAHIM.A.FLIFEL
Abstract: new ligand 5-[(2E)-2-{(2Z)-2-[2-(5-sulfanyl-1,3,4-thiadiazol-2-yl)hydrazinylidene]ethylidene}hydrazinyl]-1,3,4- thiadiazole-2-thiol with some transition metal ion such as Cr3, Co3+, Ni2+ were synthesis ,characterization by magnetic susceptibility measurements, conductance , elemental analyses, 1HNMR , FTIR , and mass spectra. The electrolytic behavior were confirmed from their conductance. data spectral study of transition metal complexes suggest octahedral geometry for Cr3+, Co3+ ion , square planer geometry for Ni2+.The effective magnetic moment of cobalt complex is 0.59that mean the Co2+ oxidation to Co3+. The complexes and ligand were tested against two types of bacteria (Staphylococcus aureus, Escherichia coli) all prepared complexes showed good biological activity.
Keyword: Thiadiazole, metal , complexes, biological activity.
DOI: https://doi.org/10.31838/ijpr/2018.10.04.079
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